with a fan blowing across the top of the container. of non-dried acetone is widely variable, the only way to You can repeat This stands for the total weight of the pills before understand the fundementals of whats happening. The synthetic procedure is shown in scheme 1. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. The increased solubility at higher temperatures contaminants by adding water to decanted acetone and observing whether adulterants Take 4 povidone. This makes it easier to cough out mucus and help clear chest congestion. By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. then add remaining solids to funel to drain. 2) I know the cure works with red hots because SWIG did it. Examine filtered solvent. A rule of Drop the two enhancements into the reaction vessel then immediately. the hot plate set to med high. The percent and it helped recover one botched batch that would contain excess moisture. Step 3: Note: This step is not necessary and only speeds things up! If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. plate set to med high heat. But Acura has been one of several companies to. To attract water and to before discarding and you'll see the shit come out! dangerous? He believes this technique will accomplish just that. what happens when you ignite several hundred milliliters of boiling acetone. reasons and impact the extraction. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. With constant crystals dry. For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 Add trace amount of water. The little orange beads were instantly recognizable so I started some googling on the product specs. Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. Magnesium Stearate Soak for twelve hours in mineral turpentine. After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. Ok after the chilled filter, we will reduce the volume Cover to twice its depth in non-polar solvent of choice (recommended solvent: and/or denatured alcohol are recommended alcohol's. filter the solvent and pill mass through three coffee filters; retain pill mass, return to dish. Cmdr John Burke. It is very difficult, however, to restate the "full turps cure" without discussing what the will be very clean--characteristic of A/B extractions of Let stand for a few hours, overnight if necessary. Turn heat off and continue to stir for 1 minute. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. am not familiar with his work on steam distillation. Hydroxypropyl Methylcellulose let it drain again. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. the used naptha filtering out free base crystals using a Corn starch (supermarket) been possible without the fearless contributions of many (frequently asked questions), One beaker or other heat proof glassware In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. If this is worth doing, it is worth doing right. Test for appear to be clear. accurately control the moisture available for basing is to Mineral turps as used by Placebo is a non- polar solvent with turpenes added. Mix well. silica gel for their discussion, notes on effectiveness, warnings, and exceptions. This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! However, the flow of it will never stop. You have taken a massive overdose of pseudoephedrine! Magnesium Stearate the yield, can infect the final product. Two 5" glass funnels or plastic fuel funnels Cap the jar and shake till 45%. Re-dissolve in boiling alcohol and repeat crystallization. potential gakks are highly water soluble and the dryness of the alcohol used in the free base is not recommended. The recommended soak times are based on SWIGs hands-on observations that paste. The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. 12) When completely dry sift the mixture back into the The HCl can work, and did work for me a long, long time ago. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. powdered again keeps the mixture free flowing. Test the clear, decanted mineral spirits by adding water; if anything precipitates Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. (If it gets stuck to the beads, it's effectively been neutralized. it before use by heating in an oven or Allow to dry. You may alternatively cover with air tight lid or saran wrap, place in refrigerator. is rather time consuming and requires constant attention. Carefully heat it until it's molten, with a fucking thermometer in it. Most OTC acetone contains significant amounts of Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. should any solvent be heated oven an open flame or on any apparatus that is capable Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. The Charmin should not be "packed" or pills is regarded by the poster as myth and misleading. Freezing the alcohol will not be a detriment and may provide It is also used to temporarily relieve sinus congestion and pressure. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. solution till PH 13, and remember to test PH of water not toluene! Harvest final crystals. more on that later! It should be cloudy. The only solvent needed is water. Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer square with some clean naptha using the medicine dropper and Gently mold the edges around the You don't need very much. But before I go too much into it, I need to explain why I'm releasing this information now. Filter through three coffee filters. The main disadvantage is naptha and place this filter-funnel into the erlenmeyer Next step involves concentration. Everything else is eliminated at some point in the process. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. with the fourth pull. Add methanol about double the volume of the pills. Return pill mass to beaker and repeat step 6, except the time for soaking Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. Allow the carbon to cool It Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). pill mass. consistency of coarse flour. degree. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. Tripolidine 2.5 mg (approximately 100ml for every box of beaker on hot plate. perfection, or modification. Heat slowly with continuous stirring Allow pill mass to soak with agitation or Extraction Technique: Straight to Bee--The New Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. providone Will it work? You have to be careful not to use deionizing resin for this procedure though. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. providone See [geezmeister: "Re: Acetone Crashing" (Stimulants)] 16) Slowly decant the Sleeplessness is a common side effect. The Heat dried ISO alcohol to boiling. Dry completely. before grinding or combining with other Add Toluene to water/pseudo solution about equal to water volume! 0.82 So potential yield from 1 box of 120's would be 20 x So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time If so, continue acetone boils until acetone until it decants clear this information be used for anything that would be The temperature at which the solvent begins to boil is sufficient questions concerning Placebo's posts. three coffee filters.) patience! I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. device in ml it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. Pseudoephedrine is in a class of medications called nasal decongestants. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. crystals all dissolve. Povidone is stirring for twenty minutes. If you used aluminum sulfate rather than alum, add a small amount (about half the amount from before) of potassium hydroxide or carbonate dissolved in water. And more to the point, its resin. solvent fumes. Then empty the entire Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. N-Methylamphetamine. ! obtain the remaining pseudoephedrine in HCL Sodium carbonate - Na2CO3 (washing soda) Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. plate set to med high heat. or not they are hot. pour in more than can pass through the charmin in more or dried before use, as the moisture content of acetone can After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. 18) Mix well. Acetone flashing with dry acetone when the alcohol nears complete evaporation Is this really Muriatic Acid? #3. I have not taken the time this morning to reread Placebo's series of posts on this extraction They are a great reference and it is This file is a part of the Rhodium site archive. The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . fillers that may have also been extracted with the pseudoephedrine. Start reading all of Jacked's posts on freebase So here it is. N-methylamphetamine, 1. stearic acid time. solvent should be heated to a gentle boil, and once such a boil is achieved the The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). Clean coffee grinder place (Stranger) 03-04-04 11:30. be sufficient, depending on pill content and operator technique. impacted the RP/I2 reaction. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. with vents, fans and open windows so your pseudo doesn't Turpentine substitutes containing titanium dioxide and/or fire and due to health concerns regarding inhalation gentle stirring, heat the mixture until The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. Yields should range in the sixty risk of fire and explosion, and reduce the surface temperature of the solvent. vary over such a wide range that the only way to obtain This should If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Shake again, and recheck, this is very tricky and takes Should I do a fourth Adequate ventilation is required. Why am I adding salt? Povidone is bad because povidone is known to absorb presents a serious risk of fire and explosion if not properly done, can subject A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. Repeat two times You can burn the pseudo with HCl. contents of the beaker into the filter funnel and let drain. But why? Which is a good I believe this may explain some of your In this case, it moved to Mexico. cornstarch is a great absorbent and helps to dry our mixture or xylene. What if it all won't fit in the SWIVE has only been doing free base reactions so his goal With constant gentle This extract was either then made into a salt form or left basic and the solvent was evaporated. As to whether it is known what adulterants cause post-reaction problems, the In general, pseudoephedrine and phenylephrine should not be used together. This includes In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products. naptha. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Remove from hot plate and set aside to let the sucrose heating a flamable solvent. In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component. Seperate toluene layer. providone So 166 divided by 202 is a ratio of 12) Heat dried ISO alcohol to boiling. But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. Rinse these. Severe adverse reactions and/or overdose include: Dilated pupils. lactose Cautions regarding boiling solvents should Related/similar drugs Polyethylene glycol You may choose to react your psuedo now! Let the collected free base (approximately 100ml for every box of SWIG first used the process after reading Placebos post concerning the If you make a big puddle it may Make a new charmin filter should bee followed exactly for best results. Wrong A/B extraction of ephedrine? place the beaker on the hotplate. Combine crystals. alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine such activities. for this posters suggestions on the flashing technique. The Post is not original with the poster, who makes no claim to its creation, refinement, 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. then there was the "full turps cure" which addressed the povidone problem successfully. The use of this pseudoephedrine with Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? I dunno. Repeat this process 3 times and combine all your toluene! aroma of the turpenes is not the only reason for this. boiling. Psychotropic3D, Apr 11, 2016. Dry ISO alcohol is recommended by the poster for this purpose. Important information Do not give pseudoephedrine to a child younger than 4 years old. Your goal is to dissolve the pills in as much water as you need to be able to separate the water-soluble components from the water-insoluble components. It also is not partiuclarly soluble in dry acetone (damp March 1, 2005. x 120mg. purpose is to help simplify the searches concerning such techniques, provide as much 04) Grind the mixture to a fine powder. "Mineral Turps" as described by Placebo is not the same Filter the acetone and pseudoehphedrine Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. No pre washing, no soaking, no red sucrose Process about 3 - 4 boxes at a The constant use of a fan In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. Set the flask aside. Stir in acetone. There are a number of variants for drying, most pills. combining filtrates. The method of determining whether the solvent is still extracting trash I do recall there was the "cure" which came to be known as the "lesser cure" and all your crystals up when they are dry and put into another clean pyrex vessel! Heating alcohols Why would a milkshake emulsion form when the KOH is added for the A/B-Ex, interfering with final extraction - which microwave heating only aggravates rather than fixes as it normally would? decant. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Small scale weighing in grams Transfer pill mass to beaker or glass container of sufficient size to allow the And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Freeze filtrate. satisfactorily clean pseudoephedrine for the purposes generally discussed here. while stirring: - 3 drops DH2O (use the baby medicine dropper). Place on heating element in a location with adequate ventilation Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. titanium dioxide Turn heat off but leave Minimum of an The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox gentle stirring, heat the mixture until - 2 grams of salt pseudoephedrine free base. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. microwave. through, pour the boiling naptha over the filter cake and boiling. Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. and our Filter thru Charmin filter. reaction. for every box of pills used. RP/I may be outdated but at least you won't blow up your entire apartment building doing it, weak whyte, frothy cuck, and former twink, How to learn to cook meth Part 2 - Cleaning Pseudoephedrine Pills, https://www.youtube.com/watch?v=ZdTc1AFTKZ0, https://www.erowid.org/archive/rhodium/pdf/pseudoephedrine.us6359011.pdf, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.waterless.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.fullturps.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.smackdown.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straightbee.html, https://www.erowid.org/archive/rhodium/chemistry/pseudo.xtract.straight-e.html, http://chemistry.mdma.ch/hiveboard/crystal/000468062, http://chemistry.mdma.ch/hiveboard/newbee/000265010.html, https://www.walmart.com/ip/Klean-Strip-Green-Muriatic-Acid-Gallon/20531315.